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冠元顆粒 |
(previous URL: http://wakandb.u-toyama.ac.jp/wiki/index.php/LCMS:Kangenkaryu)
試料情報
Voucher No. 26731
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Analytical conditions
| Instrument | Shimadzu LC-IT-TOF MS ESI |
| Column | Waters Atlantis T3 (2.1 mm x 100 mm, 3 μm) |
| Column Temperature | 40 °C |
| Solvent A | 5 mM Ammonium acetate solution |
| Solvent B | acetonitrile |
| Gradient | 10% to 100% Solvent B (0-30 min), 100% Solvent B (30-40 min), 0.15 ml/min |
| Source voltage | 4.5 kV (Positive ion mode), -3.5 kV (Negative ion mode) |
| Capillary temperature | 200 °C |
| Nebulizer gas | 1.5 l/min |
このデータを引用している論文
- Zhao Q., Matsumoto K., Tsuneyama K., Tanaka K., Li F., Shibahara N., Miyata T., Yokozawa T.: Diabetes-induced central cholinergic neuronal loss and cognitive deficit are reversed by tacrine and a Chinese herbal prescription, kangen-karyu: elucidation in type 2 diabetes db/db mice, J. Pharmacol. Sci. 117: 230-242, 2011.
https://doi.org/10.1254/jphs.11115fp